Título: | DEVELOPING A VERSATILE MONOCHROMATIZATION SYSTEM FOR X-RAYS | ||||||||||||||||||||||||||||||||||||||||
Autor: |
MARCO ROGERIO VIEIRA |
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Colaborador(es): |
GERALDO MONTEIRO SIGAUD - Orientador |
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Catalogação: | 01/JUN/2010 | Língua(s): | PORTUGUESE - BRAZIL |
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Tipo: | TEXT | Subtipo: | THESIS | ||||||||||||||||||||||||||||||||||||||
Notas: |
[pt] Todos os dados constantes dos documentos são de inteira responsabilidade de seus autores. Os dados utilizados nas descrições dos documentos estão em conformidade com os sistemas da administração da PUC-Rio. [en] All data contained in the documents are the sole responsibility of the authors. The data used in the descriptions of the documents are in conformity with the systems of the administration of PUC-Rio. |
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Referência(s): |
[pt] https://www.maxwell.vrac.puc-rio.br/projetosEspeciais/ETDs/consultas/conteudo.php?strSecao=resultado&nrSeq=15703&idi=1 [en] https://www.maxwell.vrac.puc-rio.br/projetosEspeciais/ETDs/consultas/conteudo.php?strSecao=resultado&nrSeq=15703&idi=2 |
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DOI: | https://doi.org/10.17771/PUCRio.acad.15703 | ||||||||||||||||||||||||||||||||||||||||
Resumo: | |||||||||||||||||||||||||||||||||||||||||
The investigation of the dynamics of the interaction of high-energy X-rays
and molecules of biological interest requires the energy of the X-rays to be well
defined, so that one can establish the dependence of the molecular ionization and
fragmentation patterns as functions of the incident beam energy. For this
purpose, a versatile system for the monochromatization of the broadband beams
produced by an ISOVOLT 160M2 X-ray tube has been designed, constructed
and characterized. The monochromator consists of a pair of crystals mounted on
two translator tables fixed on a high-precision goniometer, all manufactured by
Newport Corp. This configuration allows independent translational motions for
the two crystals, associated to a rotational motion of the whole system in respect
to the direction of the incident X-ray beam. These motions, together with a
convenient choice of the pair of crystals for a given energy range - which
depends on the material and orientation of the crystals -, will allow us to cover a
wide range of X-rays energies, roughly from few to around 100 keV. However,
it has not yet been possible to distinguish energy-defined X-ray peaks with the
complete two-crystal system. Some of the possible causes may be related to the
large angular dispersion of the incident beam and to the need of more accurate
adjustments of the parallelism between both crystals. When this system is fully
operational, it will be possible to perform a large variety of experiments in the
fields of collision and radiation physics, such as, molecular fragmentation by Xrays,
selective fluorescence and diffraction in crystals, real-time evaluation of Xray-
induced damage in biological tissues, non-destructive testing of materials,
among many other aplications.
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