This thesis aims to establish a methodology for the metrological characterization of Bragg gratings type I, type II and type regenerated statistically thereby estimating and validating the measurement results for high temperature sensing applications. Beyond telecommunications applications, optical fibers are still used for optical sensing, since the silica fiber has great optical efficiency for data transmission. The growing demand for high-temperature measurements in industrial processes has enabled the development of new measurement technologies beyond the traditional technologies already in use today. Thus were created the conditions necessary to introduce a new technology of temperature measurement with Bragg gratings which presents some advantages compared with traditional technologies of measurement. Although there are several prior studies none of those examined the by others about temperature measurement with Bragg gratings, metrological issues, and is particular, the estimate of the measurement uncertainties surrounding the whole process of measurement and characterization of Bragg gratings at high temperature. The adaptation of a traditional system of calibration instruments for temperature measurement was developed and designed in such a way that allowed the characterization of different types of gratings. It was observed that the measurement results and the estimated uncertainties of the measurements obtained for all gratings, successfully approached the theoretical models used, confirming the adequacy of the measurement of temperature and optical sensing.